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Beilstein J. Org. Chem. 2018, 14, 3011–3017, doi:10.3762/bjoc.14.280
Graphical Abstract
Figure 1: Synthesis of mono- or dialkylated acetonitriles.
Figure 2: Cyanation through 5-chloromethyl-3-(p-substituted-phenyl)-1,2,4-oxadiazole.
Figure 3: Expanded HSQC spectrum of 4a and 3a.
Figure 4: X-ray ORTEP plots of 3a and 4e.
Scheme 1: Plausible mechanism for the formation of 3.
Scheme 2: Plausible mechanism for the formation of 4 via decyanation of 3.